- Chemical Name 2-phenyl-1,3-dioxane
- CAS No. 772-01-0
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- Molecular Formula: C10H12 O2
- Molecular Weight: 164.204
- Vapor Pressure: 0.0298mmHg at 25°C
- Melting Point: 41°C
- Refractive Index: 1.5155 (estimate)
- Boiling Point: 253°C at 760 mmHg
- Flash Point: 113.2°C
- PSA： 18.46000
- Density: 1.075g/cm3
- LogP: 2.12210
2-phenyl-1,3-dioxane(Cas 772-01-0) Usage
|
Synthesis Reference(s) |
Tetrahedron Letters, 16, p. 4543, 1975 DOI: 10.1016/S0040-4039(00)91066-9 |
InChI:InChI=1/C10H12O2/c1-2-5-9(6-3-1)10-11-7-4-8-12-10/h1-3,5-6,10H,4,7-8H2
772-01-0 Relevant articles
An Intramolecular Iodine-Catalyzed C(sp3)?H Oxidation as a Versatile Tool for the Synthesis of Tetrahydrofurans
Br?se, Stefan,Koch, Vanessa
supporting information, p. 3478 - 3483 (2021/07/22)
The formation of ubiquitous occurring te...
Phosphotungstic Acid Supported on Magnetic Mesoporous Tantalum Pentoxide Microspheres: Efficient Heterogeneous Catalysts for Acetalization of Benzaldehyde with Ethylene Glycol
Feng, Caiting,Li, Qinlong,Wu, Panfeng,Liu, Bin,Hu, Huaiming,Xue, Ganglin
, p. 1204 - 1217 (2019/11/19)
Abstract: In this study, magnetically-re...
Direct anodic (thio)acetalization of aldehydes with alcohols (thiols) under neutral conditions, and computational insight into the electrochemical formation of the acetals
Liu, Caiyan,Shen, Yongli,Xiao, Zihui,Yang, Hui,Han, Xue,Yuan, Kedong,Ding, Yi
, p. 4030 - 4034 (2019/08/07)
A versatile protocol for the production ...
A Direct Method for the Efficient Synthesis of Benzylidene Acetal at Room Temperature
Reddy, Narra Rajashekar,Kumar, Rashmi,Baskaran, Sundarababu
supporting information, p. 1548 - 1552 (2019/01/09)
For the first time, a metal-free direct ...
772-01-0 Process route
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-
1439-07-2
trans-Stilbene oxide
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-
504-63-2
trimethyleneglycol
-
-
772-01-0
2-phenyl-1,3-dioxane
-
-
492-70-6,655-48-1,2325-10-2,38270-73-4,52340-78-0,579-43-1
1,2-diphenyl-1,2-ethanediol
-
-
100-52-7
benzaldehyde
| Conditions | Yield |
|---|---|
|
With
PTAB; antimony(III) bromide;
In
dimethyl sulfoxide;
at 20 ℃;
for 40h;
Further Variations:;
Reagents;
Solvents;
reaction times, reagent ratios;
Product distribution;
|
71%
|
-
-
1689-71-0
cis-1,2-diphenyloxirane
-
-
504-63-2
trimethyleneglycol
-
-
772-01-0
2-phenyl-1,3-dioxane
-
-
492-70-6,655-48-1,2325-10-2,38270-73-4,52340-78-0,579-43-1
1,2-diphenyl-1,2-ethanediol
| Conditions | Yield |
|---|---|
|
With
PTAB; antimony(III) bromide;
In
dimethyl sulfoxide;
at 20 ℃;
|
60%
9% |
772-01-0 Upstream products
-
75526-35-1
2-Phenyl-4H -[1,3]dioxin
-
100-52-7
benzaldehyde
-
504-63-2
trimethyleneglycol
-
1125-88-8
benzaldehyde dimethyl acetal
772-01-0 Downstream products
-
4799-68-2
3-benzyloxypropan-1-ol
-
10601-29-3
5,5,7-Tris-
-8,8,8-trifluor-4,6-dioxa-octyl-benzoat -
942-95-0
3-chloropropyl benzoate
-
67516-70-5
2-dichloromethyl-2-phenyl-[1,3]dioxane